Synthesis, characterization, computational studies, antimicrobial activities and carbonic anhydrase inhibitor effects of 2-hydroxy acetophenone-N-methyl p …
Yazarlar (6)
Prof. Dr. Neslihan ÖZBEK Türkiye
Saliha Alyar
Burcu Koçak Memmi
Ayla Balaban Gündüzalp
Zafer Bahçeci
Hamit Alyar Kırşehir Ahi Evran Üniversitesi
| Makale Türü | Özgün Makale (Uluslararası alan indekslerindeki dergilerde yayınlanan tam makale) | ||
| Dergi Adı | Journal of Molecular Structure | ||
| Makale Dili | – | Basım Tarihi | 01-2017 |
| Cilt / Sayı / Sayfa | 1127 / 0 / 437–448 | DOI | – |
| Makale Linki | https://www.sciencedirect.com/science/article/pii/S002228601630816X | ||
| UAK Araştırma Alanları |
Anorganik Kimya
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| Özet |
| 2-Hydroxyacetophenone-N-methyl p-toluenesulfonylhydrazone (afptsmh) derived from p-toluenesulfonicacid-1-methylhydrazide (ptsmh) and its Co(II), Pd(II), Pt(II) complexes were synthesized for the first time. Synthesized compounds were characterized by spectroscopic methods (FT-IR, 1Hsingle bond13C NMR, LC-MS, UV–vis), magnetic susceptibility and conductivity measurements. 1H and 13C shielding tensors for crystal structure of ligand were calculated with GIAO/DFT/B3LYP/6-311++G(d,p) methods in CDCl3. The vibrational band assignments were performed at B3LYP/6-311++G(d,p) theory level combined with scaled quantum mechanics force field (SQMFF) methodology. The antibacterial activities of synthesized compounds were studied against some Gram positive and Gram negative bacteria by using microdilution and disc diffusion methods. In vitro enzyme inhibitory effects of the compounds were … |
| Anahtar Kelimeler |
