High-resolution continuum source flame atomic absorption spectrometric (HR-CS FAAS) determination of trace aluminium and lead in water and some beverage samples after separation and preconcentration procedure
Yazarlar (5)
Prof. Dr. Harun ÇİFTÇİ Kırşehir Ahi Evran Üniversitesi, Türkiye
Doç. Dr. Çiğdem ER ÇALIŞKAN Kırşehir Ahi Evran Üniversitesi, Türkiye
Özcan Yalçınkaya Gazi Üniversitesi, Türkiye
Mehmet Mürşit Temüz Fırat Üniversitesi, Türkiye
Ali Rehber Türker
Gazi Üniversitesi, Türkiye
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı International Journal of Environmental Analytical Chemistry (Q3)
Dergi ISSN 0306-7319 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Makale Dili İngilizce Basım Tarihi 12-2014
Kabul Tarihi 12-04-2026 Yayınlanma Tarihi
Cilt / Sayı / Sayfa 94 / 6 / 579–593 DOI 10.1080/03067319.2013.864646
Makale Linki https://doi.org/10.1080/03067319.2013.864646
Özet
In the present study, a solid phase extraction procedure has been presented for the separation and preconcentration of aluminium (Al) and lead (Pb) in various matrixes such as water, cola and fruit juice samples. 4-[(3-amino-5-{[(2-hydroxyphenyl) methylidene] amino}-1H-pyrazol-4-yl) diazenyl] benzoic acid (AHPMAPDAB) was used as a ligand. AHPMAPDAB chelates of Al and Pb ions in aqueous solutions were adsorbed on polystyrene-graft-ethyl methacrylate copolymer (Poly S15-g-EMA120). Various experimental and analytical parameters such as sample solution pH, sample volume, flow rate of sample solution and eluent, volume and concentration of eluent, amount of ligand and adsorbent, effect of common matrix ions and capacity of adsorbent were investigated. The adsorbed metal ions on resin were eluted with 6 mL of 2 mol L−1 HCl solutions and their concentrations were determined by high-resolution …
Anahtar Kelimeler
aluminium | beverages | continuum source atomic absorption spectrometry | graft polymer | lead | preconcentration