Enrichment and determination of Ni2 ions in water samples with a diamino 4 4 nitro phenylazo 1H pyrazole PDANP by using FAAS
Yazarlar (5)
Prof. Dr. Harun ÇİFTÇİ Kırşehir Ahi Evran Üniversitesi, Türkiye
Erdal Eren Bilecik Şeyh Edebali Üniversitesi, Türkiye
Ali Ölçücü Fırat Üniversitesi, Türkiye
Memet Şekerci Fırat Üniversitesi, Türkiye
Halil Yalçın Firat Üniversitesi
Makale Türü Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı Desalination
Dergi ISSN 0011-9164 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler SCI-Expanded
Makale Dili İngilizce Basım Tarihi 06-2010
Kabul Tarihi 12-04-2026 Yayınlanma Tarihi
Cilt / Sayı / Sayfa 256 / 1 / 48–53 DOI 10.1016/j.desal.2010.02.018
Makale Linki http://linkinghub.elsevier.com/retrieve/pii/S0011916410000950
Özet
Nickel, as a heavy metal, is toxic for many living species. Thus, the determination of trace amounts of nickel in environmental samples is of great importance. In the present study, new, sensitive, simple and validated solid phase extraction method is developed for the determination of nickel. In recent study nickel was preconcentrated as diamino-4-(4-nitro-phenylazo)- 1H-pyrazole (PDANP) chelates (Ni-PDANP) from sample solutions using a column containing Amberlite XAD-7 and determined by flame atomic absorption spectrometry (FAAS). The optimum experimental parameters such as pH of the medium, sample flow rate, eluent and effect of matrix ions on the method efficiency were investigated. The optimum pH value for quantitative sorption of Ni–PDANP was found between 6.0 and 8.0. Elution process was performed by using 6mL of 2molL−1 HCl. The sorption capacity of resin was determined to be 7.2mgg−1 …
Anahtar Kelimeler
Amberlite XAD-7 | FAAS | Nickel | PDANP | Preconcentration | Solid phase extraction