Optimization of Analytical Parameters for Determination of Iron Nickeland Cobalt in Plants with RP HPLC

ÇİFTÇİ, HARUN; Ölçücü, Ali; Özkaya, Ahmet; Çiftçi, Tacettin

Optimization of Analytical Parameters for Determination of Iron Nickeland Cobalt in Plants with RP HPLC

Yazarlar (4)

Prof. Dr. Harun ÇİFTÇİ Kırşehir Ahi Evran Üniversitesi, Türkiye

Ali Ölçücü
Kırşehir Ahi Evran Üniversitesi, Türkiye

Ahmet Özkaya
Kırşehir Ahi Evran Üniversitesi, Türkiye

Tacettin Çiftçi
Kırşehir Ahi Evran Üniversitesi, Türkiye

Makale Türü	Özgün Makale (SSCI, AHCI, SCI, SCI-Exp dergilerinde yayınlanan tam makale)
Dergi Adı	Asian Journal of Chemistry (Q4)
Dergi ISSN	0970-7077 Wos Dergi Scopus Dergi
Dergi Tarandığı Indeksler	SCI-Expanded
Makale Dili	İngilizce	Basım Tarihi	01-2009
Cilt / Sayı / Sayfa	21 / 4 / 2643–2652	DOI	–

Özet

This study optimized the analytical parameters such as combination of mobile phase, pH of mobile phase, attempt effect of strange ions and current rate for simultaneous determination of iron, nickel and cobalt. 4-(2-Pyridiylazo)resorcinol (PAR) ligand is used for metal chelates. The metal-PAR chelates were separated on a Luna C18 siloxane bonded phase and eluted within 7.4 min of Co-PAR, 9.6 min of Fe-PAR and 12.4 min of Ni-PAR with methanol-water-acetonitrile-(l × 10'² mol L"¹) sodium acetate (55:40:2.5:2.5 v/v) (pH 5.3). Detection limits of process for Fe- PAR, Ni-PAR and Co-PAR under optimized conditions (500 nm) were found as 4.45,3.26 and 1.86 μg L^-1 respectively. The analysis of Fe, Ni and Co ions in plant samples under optimized conditions were carried out by HPLC.

Anahtar Kelimeler

BM Sürdürülebilir Kalkınma Amaçları

Atıf Sayıları
WoS	12
SCOPUS	13
Google Scholar	16

Dergi Adı	ASIAN JOURNAL OF CHEMISTRY
Yayıncı	Asian Publication Corporation
Açık Erişim	Hayır
ISSN	0970-7077
E-ISSN	0975-427X
CiteScore	0,8
SJR	0,156
SNIP	0,157

Optimization of Analytical Parameters for Determination of Iron Nickeland Cobalt in Plants with RP HPLC

Paylaş